Effect of curing mode on micro tensile bond strength of resin composite cements
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Abstract
Objectives: To investigate the micro-tensile bond strength (μTBS) to dentin of resin composite cements in different curing modes.
Materials and Methods: The μTBS of three resin composite cements—Panavia V5 (PV), Panavia SA Universal (SA), and RelyX Universal (RXU)— bonded to dentin were tested in two curing modes. PV was evaluated in auto polymerization (AA) and co-curing (AL) modes, while SA and RXU were tested in AL and separate light-curing (LL) modes. Failure modes were analyzed by light microscopy and SEM. Data were analyzed using one-way ANOVA and Tukey’s post hoc test (p<0.05).
Results: PV had the highest bond strength, with no significant difference between AA and AL modes. In contrast, SA and RXU showed significantly lower μTBS in AL than LL. High rates of pretesting failures and adhesive failure modes were observed in the co-curing groups of SA and RXU. SEM analysis revealed voids and signs of water infiltration at the adhesive-dentin interface.
Conclusion: Co-curing adhesive-assisted resin composite cements (SA, RXU) significantly reduced bond strength. Primer-assisted resin composite cement (PV) maintained high bond strength across both curing modes.
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References
Maravic T, Mazzitelli C, Mancuso E, Del Bianco F, Josic U, Cadenaro M, et al. Resin composite cements: Current status and a novel classification proposal. J Esthet Restor Dent. 2023 Oct;35(7):1085-1097. doi:10.1111/jerd.13036.
Luhrs AK, De Munck J, Geurtsen W, Van Meerbeek B. Composite cements benefit from light-curing. Dent Mater. 2014 Mar;30(3):292-301.doi:10.1016/j.dental.2013.11.012.
Luhrs AK, Pongprueksa P, De Munck J, Geurtsen W, Van Meerbeek B. Curing mode affects bond strength of adhesively luted composite CAD/CAM restorations to dentin. Dent Mater. 2014 Mar;30(3):281-291.doi:10.1016/j.dental.2013.11.016.
Kawano S, Fu J, Saikaew P, Chowdhury AA, Fukuzawa N, Kadowaki Y, et al. Microtensile bond strength of a newly developed resin cement to dentin. Dent Mater J. 2015;34(1):61-69. doi:10.4012/dmj.2014-122
Yoshihara K, Nagaoka N, Benino Y, Nakamura A, Hara T, Maruo Y, et al. Touch-cure polymerization at the composite cement-dentin Interface. J Dent Res. 2021 Aug;100(9):935-942. doi: 10.1177/00220345211001020.
Armstrong S, Breschi L, Ozcan M, Pfefferkorn F, Ferrari M, Van Meerbeek B. Academy of dental materials guidance on in vitro testing of dental composite bonding effectiveness to dentin/enamel using micro-tensile bond strength (muTBS) approach. Dent Mater. 2017 Feb;33(2):133-143. doi: 10.1016/j.dental.2016.11.015.
Pratap B, Gupta R, Bhardwaj B, Nag M. Resin based restorative dental materials: characteristics and future perspectives. Jpn Dent Sci Rev. 2019 Nov;55(1):126-138. doi:10.1016/j.jdsr.2019.09.004.
Chimeli TB, D'Alpino PH, Pereira PN, Hilgert LA, Di Hipólito V, Garcia FC. Effects of solvent evaporation on water sorption/solubility and nanoleakage of adhesive systems. J Appl Oral Sci. 2014 Jul-Aug;22(4):294-301. doi: 10.1590/1678-775720130653.
Son SA, Kim JH, Seo DG, Park JK. Effect of dentin surface conditions and curing mode of resin cement on the dentin bond strength. Dent Mater J. 2024 Jun;43(3):469-476. doi:10.4012/dmj.2023-287.
Vukelja J, Klarić Sever E, Sever I, Jukić Krmek S, Tarle Z. Effect of conventional adhesive application or co-curing technique on dentin bond strength. Materials (Basel). 2021 Dec;14(24) :7664.doi: 10.3390/ma14247664.
Dimitriadi M, Petropoulou A, Zinelis S, Eliades G. Degree of conversion of dual-cured composite luting agents: The effect of transition metal-based touch-cure activators. J Dent. 2024 Aug;147:105147. doi: 10.1016/j.jdent.2024.105147.
Garra P, Kermagoret A, Al Mousawi A, Dumur F, Gigmes D, Morlet-Savary F, et al. New copper(i) complex based initiating systems in redox polymerization and comparison with the amine/benzoyl peroxide reference. Polym. Chem. 2017;8(28):4088-4097. doi:10.1039/C7PY00726D.
Ozaki A, Shishido S, Nakamura K, Harada A, Katsuda Y, Kanno T, et al. Impact of adhesive primer and light-curing on polymerization kinetics of self-adhesive resin cement in association with free radical reaction. Eur J Oral Sci. 2021 Dec;129(6):e12828. doi:10.1111/eos.12828.
Gresnigt M, Özcan M, Muis M, Kalk W. Bonding of glass ceramic and indirect composite to non-aged and aged resin composite. J Adhes Dent. 2012 Feb;14(1):59-68. doi:10.3290/j.jad.a21418.
Ferracane JL, Stansbury JW, Burke FJ. Self-adhesive resin cements - chemistry, properties and clinical considerations. J Oral Rehabil. 2011 Apr;38(4):295-314. doi:10.1111/j.1365-2842.2010.02148.x.